Equipment

• UV-Vis spectrophotometer with temperature controlled sample holder and temperature controller (Shimadzu UV3600; range: 3600-185 nm)

• UV-Vis spectrophotometer (Perkin Elmer Lambda800)

• IR spectrometer (Shimadzu IR-Affinity; range 7800 - 350 cm^–1)

• IR spectrometer (Perkin-Elmer System 2000)

• X-ray diffractometer with molybdenum radiation and temperature control for structural analysis of small molecules (STOE IPDS2T)

• X-ray diffractometer with copper radiation and temperature control for structural analysis of small molecules and proteins (Rigaku XtaLAB Synergy; co-usage only)

• Elemental Analyzer from Elementar (C, H, N, and S; Vario Micro Cube)

• 400 MHz NMR (Jeol) – all NMR-active nuclei and various methods (correlations, 2D, kinetics etc.)  see page NMR-Service unter heading 'Messangebot': NMR-Service

• Mass spectrometer for FAB and EI (AMD40, AMD Intectra)

• A mass spectrometer shared with three other groups: compact-ESI-MS „Advion expression CMS“

• Glovebox with <0.1 ppm water and < 0.1 ppm O2 ; SPS with thf and acetonitrile (MBraun)

• Electrochemistry with temperature control; can be run inside a glovebox (Metrohm Potentiostat/Galvanostat PG12)

• HPLC (Knauer, Smartline, 2006)

• Gaschromatograph (Hewlett Packard 5890 Series II)

• Microwave with pressure and temperature control (MLS-MW-System)

• Photochemical equipment (for photolysis, activation etc.; two lamps: HPA with 1200 Watt power and HPM with 1100 Watt power)

• Interchim Ultra Performance Flash Purification System puriFlash 5.020 (Flash Chromatography)

_{aktualisiert am 29.05.2026 durch Prof. Dr. C. Schulzke}