Equipment


  • UV-Vis spectrophotometer with temperature controlled sample holder and temperature controller (Shimadzu UV3600; range: 3600-185 nm)
     
  • UV-Vis spectrophotometer (Perkin Elmer Lambda800)
     
  • IR spectrometer (Shimadzu IR-Affinity; range 7800 - 350 cm–1)
     
  • IR spectrometer (Perkin-Elmer System 2000)
     
  • X-ray diffractometer with molybdenum radiation and temperature control for structural analysis of small molecules (STOE IPDS2T)
     
  • Elemental Analyzer from Elementar (C, H, N, and S; Vario Micro Cube)
     
  • 300 MHz NMR (Bruker AVANCE) – for nuclei and methods see page NMR-Service unter heading 'Messangebot': NMR-Service
     
  • Mass spectrometer for FAB and EI (AMD40, AMD Intectra)
     
  • A mass spectrometer shared with three other groups: compact-ESI-MS „Advion expression CMS“
     
  • Glovebox with <0.1 ppm water and < 0.1 ppm O2 ; SPS with thf and acetonitrile (MBraun)
     
  • Electrochemistry with temperature control; can be run inside a glovebox (Metrohm Potentiostat/Galvanostat PG12)
     
  • HPLC (Knauer, Smartline, 2006)
     
  • Gaschromatograph (Hewlett Packard 5890 Series II)
     
  • Microwave with pressure and temperature control (MLS-MW-System)
  • Photochemical equipment (for photolysis, activation etc.; two lamps: HPA with 1200 Watt power and HPM with 1100 Watt power)
  • Interchim Ultra Performance Flash Purification System puriFlash 5.020 (Flash Chromatography)

 

aktualisiert am 18.03.2020 durch Prof. Dr. C. Schulzke